Organic Structure Analysis


Author: Phillip Crews,Jaime Rodríguez,Marcel Jaspars
Publisher: Oxford University Press, USA
ISBN: 9780195336047
Category: Medical
Page: 636
View: 3978

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The most up-to-date integrated spectroscopy text available, Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis, organic structure identification, and organic spectroscopy, it emphasizes real applications--integrating theory as needed--and introduces students to the latest spectroscopic methods. An Instructor's Resource CD-ROM, which includes all of the figures from the text in electronic format and the solutions to all of the exercises and problems from the text (in an editable Word file format), is also available for adopting professors. Please contact your publisher sales representative. FEATURES * Focus on Structure: Opens with structural elements and then considers the characteristics, advantages, and disadvantages of spectroscopic methods. Includes coverage of the steps used in determining a molecular structure, the limitations to organic structure determination by spectroscopic methods, and an "Organic Structure Analyses Gone Bad" table (all unique to this text) * Practical Organization: Presents the most commonly used methods first, beginning with an overview of strategies, followed by the use of NMR, and then moving on to mass spectrometry, infrared, and ultraviolet * Innovative Real-World Problem-Solving Approach: Follows the actual information flow used by chemists to solve molecular structures, as opposed to the standard methods-based approach of other texts * Unique Chapter (12) Featuring 51 Structure-Solving Problems: Each problem emphasizes a different method; the problems increase in difficulty throughout the chapter, successively building on students' knowledge and requiring them to integrate multiple methods to identify molecules. NEW TO THE SECOND EDITION * Coverage of the Latest Instrumental and Computational Advances: Examines the use of modern instruments, data processing, and computer-assisted structure elucidation techniques * Updated and Expanded Treatment of NMR (Chapters 2-5): An extensively revised Chapter 5 discusses multi-pulse 1D and 2D NMR methods, 1D TOCSY and 1D NOESY sequences, and using NOESY and ROESY in determining relative stereochemistry and solution conformation. * Additional Coverage of Mass Spectrometry: A new chapter (7) expands the discussion of mass spectrometry to three chapters (6-8). Topics include cutting-edge MS instrumentation and new information on tandem MS techniques, combining NMR with MS, large-molecule MS, chemo-informatics, and more. * More Exercises and Improved Spectra: The second edition includes 25% more problems than the previous edition (279 total). In addition, many of the spectra, including all of those presented in Chapters 11 and 12, have been reprocessed or reacquired for greater clarity.

Organic Structure Analysis


Author: Phillip Crews,Jaime Rodríguez,Marcel Jaspars
Publisher: Oxford University Press, USA
ISBN: 9780195101027
Category: Science
Page: 552
View: 8789

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Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage, it is the only text that emphasizes strategies, interpretation, modern techniques, and problem solving. The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements. Organic Structure Analysis adopts a practical approach to the subject which emphasizes building experience; the authors recognize that a combination of problem solving, access to data from models, and understanding the rules of spectral interpretation helps students to build expertise in structure determination from spectra. It outlines elements of theory, but with an emphasis on those directly relevant to spectral interpretation. The text is divided into three major sections: the first section provides extensive coverage of each of the individual methods, the second section illustrates how the strategies of organic structure analysis are actually applied in ten problems whose solutions are provided, and the third section consists of fifty unsolved problems which range from simple monofunctional compounds to complex natural products.

Organic Structure Analysis

Chemistry, Organic chemistry
Author: CTI Reviews
Publisher: Cram101 Textbook Reviews
ISBN: 1478451580
Category: Education
Page: 71
View: 475

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Facts101 is your complete guide to Organic Structure Analysis. In this book, you will learn topics such as INTERPRETATION AND USE OF PROTON AND CARBON CHEMICAL SHIFTS, INTERPRETATION AND USE OF PROTON AND CARBON COUPLING CONSTANTS, MULTIPLE-PULSE AND MULTIDIMENSIONAL NMR TECHNIQUES, and MASS SPECTROMETRY: CORE TECHNIQUES AND IONIZATION PROCESSES plus much more. With key features such as key terms, people and places, Facts101 gives you all the information you need to prepare for your next exam. Our practice tests are specific to the textbook and we have designed tools to make the most of your limited study time.

Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods


Author: J.T. Clerc,E. Pretsch,J. Seibl
Publisher: Elsevier
ISBN: 0444597549
Category: Science
Page: 288
View: 2924

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Structural Analysis of Organic Compounds covers some practical analytical aspects of organic structural analysis by combined application of spectroscopic methods. This book is composed of three parts encompassing 35 chapters that specifically describe infrared-, ultraviolet-, proton and carbon-13 nuclear magnetic resonance and mass spectroscopy. Considerable chapters discuss the problems intended to cover a wide variety of chemical structure and spectroscopic argument, thereby exemplifying interpretations and comment on specific practical aspects of the problem solving procedure. The remaining chapters provide short supplementing research concerning various aspects of structural analysis. This book will prove useful to organic and analytical chemists.

Problems in Organic Structure Determination

A Practical Approach to NMR Spectroscopy
Author: Roger G. Linington,Philip G. Williams,John B. MacMillan
Publisher: CRC Press
ISBN: 1498719635
Category: Science
Page: 755
View: 6363

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At a point where most introductory organic chemistry texts end, this problems-based workbook picks up the thread to lead students through a graduated set of 120 problems. With extensive detailed spectral data, it contains a variety of problems designed by renowned authors to develop proficiency in organic structure determination. This workbook leads you from basic problems encountered in introductory organic chemistry textbooks to highly complex natural product-based problems. It presents a concept-based learning platform, introducing key concepts sequentially and reinforcing them with problems that exemplify the complexities and underlying principles that govern each concept. The book is organized in such a way that allows you to work through the problems in order or in selections according to your experience and desired area of mastery. It also provides access to raw data files online that can be downloaded and used for data manipulation using freeware or commercial software. With its problem-centered approach, integrated use of online and digital resources, and appendices that include notes and hints, Problems in Organic Structure Determination: A Practical Approach to NMR Spectroscopy is an outstanding resource for training students and professionals in structure determination.

Determination of Organic Structures by Physical Methods


Author: E. A. Braude,F. C. Nachod
Publisher: Elsevier
ISBN: 1483275728
Category: Science
Page: 824
View: 8717

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Determination of Organic Structures by Physical Methods, Volume 1 focuses on the processes, methodologies, principles, and approaches involved in the determination of organic structures by physical methods, including infrared light absorption, thermodynamic properties, Raman spectra, and kinetics. The selection first elaborates on the phase properties of small molecules, equilibrium and dynamic properties of large molecules, and optical rotation. Discussions focus on simple acyclic compounds, carbohydrates, steroids, diffusion, viscosity, osmotic pressure, sedimentation velocity, melting and boiling points, and molar volume. The book then examines ultraviolet and visible light absorption, infrared light absorption, Raman spectra, and the theory of magnetic susceptibility. Concerns cover applications to the study of organic compounds, applications to the determination of structure, determination of thermodynamic properties, and experimental methods and evaluation of data. The text ponders on wave-mechanical theory, reaction kinetics, and dissociation constants, including dissociation of molecular addition compounds, principles of reaction kinetics, and valence-bond treatment of aromatic systems. The selection is a valuable source of data for researchers interested in the determination of organic structures by physical methods.

Organische Chemie


Author: Kurt Peter C. Vollhardt,Neil Eric Schore
Publisher: John Wiley & Sons
ISBN: 3527327541
Category: Chemistry, Organic
Page: 1452
View: 7210

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Besser Konzepte und Ideen der organischen Chemie verstehen, als eine Vielzahl von Fakten auswendig beherrschen! Diesem Motto bleibt der "Vollhardt/Schore" auch in der neuesten Auflage treu. Das neu gestaltete Layout, beispielhaft gelöste Übungsaufgaben und die deutlich erweiterten Verständnisübungen führen einprägsam an die Methodik zur Lösung organisch-chemischer Probleme heran. So werden nicht nur die stofflichen Grundlagen der organischen Chemie, sondern auch das "Gewusst wie" fast schon spielerisch vermittelt. Nicht nur für Chemiestudenten, auch für Biochemiker, Pharmazeuten, Biologen und Mediziner ist der "Vollhardt/Schore" der fachliche Grundstock für die organische Chemie.

X-ray analysis and the structure of organic molecules


Author: Jack D. Dunitz
Publisher: Cornell Univ Pr
ISBN: N.A
Category: Science
Page: 514
View: 6780

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Jack D. Dunitz X-Ray Analysis and the Structure of Organic Molecules From the Reviews of the First Edition ÊThe book may be recommended most heartily to anyone who would like to know how molecular structures are determined and what can be deduced from them apart from their topology. The author is evidently a great admirer of the method and its results. The reviewer would agree that Êcooking' is not the only way to bring chemically relevant knowledge to light.' Angew. Chem., Int. Ed. ÊAll the information in this text is of considerable value especially to those engaged in, or about to embark upon, X-ray crystal structure analysis but even more so, perhaps, to the non-specialist who may now proceed profitably and discriminately to read the explosively growing crystallographic literature. The author has certainly succeeded in taking us not only on a guided tour, but at the same time has provided rather more of the kind of detail one expects in the best guidebooks.' Int. Rev. Phys. Chem. ÊAll crystallographers, whatever their special structural interests, should get a copy and keep it by them, and many research supervisors will be very happy to entrust their research students to such a sound and stimulating guide.' Chem. in Britain

Experimental Organic Chemistry: A Miniscale and Microscale Approach


Author: John C. Gilbert,Stephen F. Martin
Publisher: Cengage Learning
ISBN: 1111789266
Category: Science
Page: 960
View: 7118

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Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin's proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as small scale) and microscale users. The manual first covers equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.

Organische Chemie


Author: Jonathan Clayden,Nick Greeves,Stuart Warren
Publisher: Springer Spektrum
ISBN: 9783642347153
Category: Science
Page: 1366
View: 9989

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Ein neuer Stern am Lehrbuch-Himmel: Organische Chemie von Clayden, Greeves, Warren - der ideale Begleiter für alle Chemiestudenten. Der Schwerpunkt dieses didaktisch durchdachten, umfassenden vierfarbigen Lehrbuches liegt auf dem Verständnis von Mechanismen, Strukturen und Prozessen, nicht auf dem Lernen von Fakten. Organische Chemie entpuppt sich als dabei als ein kohärentes Ganzes, mit zahlreichen logischen Verbindungen und Konsequenzen sowie einer grundlegenden Struktur und Sprache. Dank der Betonung von Reaktionsmechanismen, Orbitalen und Stereochemie gewinnen die Studierenden ein solides Verständnis der wichtigsten Faktoren, die für alle organisch-chemischen Reaktionen gelten. So lernen sie, auch Reaktionen, die ihnen bisher unbekannt waren, zu interpretieren und ihren Ablauf vorherzusagen. Der direkte, persönliche, studentenfreundliche Schreibstil motiviert die Leser, mehr erfahren zu wollen. Umfangreiche Online-Materialien führen das Lernen über das gedruckte Buch hinaus und vertiefen das Verständnis noch weiter.

Structure Elucidation in Organic Chemistry

The Search for the Right Tools
Author: Maria-Magdalena Cid,Jorge Bravo (chemik)
Publisher: John Wiley & Sons
ISBN: 3527333363
Category: Science
Page: 552
View: 6961

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A major challenge in structural analysis is not only the structures of single molecules, but also their interactions. This book is intended for advanced readers, and reviews all relevant techniques for structure analysis in one handy volume. It provides the latest knowledge on spectroscopic and related techniques for chemical structure analysis, such as NMR, optical spectroscopy, mass spectrometry and X-ray crystallography, with particular emphasis on the scope and limitation of each method. Readers will not only become acquainted with the techniques, but also the advantages of the synergies between them, enabling a time- and resource efficient choice of analytical method for each problem to be made. Special emphasis is placed on NMR and its application to absolute configuration determination and the analysis of molecular interactions. Adopting a practical point of view, the author team from academia and industry guarantees both solid methodology and applications essential for structure determination, equipping experts as well as newcomers with the tools to solve any structural problem.

Organic Structures from Spectra


Author: L. D. Field,S. Sternhell,John R. Kalman
Publisher: John Wiley & Sons
ISBN: 111996461X
Category: Science
Page: 468
View: 8825

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Organic Structures from Spectra, Fourth Edition consists of a carefully selected set of over 300 structural problems involving the use of all the major spectroscopic techniques. The problems are graded to develop and consolidate the student’s understanding of Organic Spectroscopy, with the accompanying text outlining the basic theoretical aspects of major spectroscopic techniques at a level sufficient to tackle the problems. Specific changes for the new edition will include A significantly expanded section on 2D NMR spectroscopy focusing on COSY, NOESY and CH-Correlation Incorporating new material into some tables to provide extra characteristic data for various classes of compounds Additional basic information on how to solve spectroscopic problems Providing new problems within the area of 10 2D NMR spectroscopy More problems at the ‘simpler’ end of the range As with previous editions, this book combines basic theory, practical advice and sensible approaches to solving spectra problems. It will therefore continue to prove invaluable to students studying organic spectroscopy across a range of disciplines.

Modern Conformational Analysis

Elucidating Novel Exciting Molecular Structures
Author: Helena Dodziuk
Publisher: John Wiley & Sons
ISBN: 9780471186113
Category: Science
Page: 276
View: 937

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Most books on organic conformational deal with sterochemistry, while neglecting the spatial structure of organic molecules, especially the unusual ones. This ambitious monograph presents a global view of organic structure and conformational analysis in a very readable style. The author's fascination with the beauty and variety of shapes of organic molecules comes through in her description of the importance of molecular organization in organic chemical and biological systems, the quantum foundations of molecular spatial structure, molecular symmetry, chiralty and physical methods for studying molecular geometry. She provides ample bases for the new trends in organic conformational chemistry, including the application of Computer Assisted Molecular Design (CAMD) to organic synthesis.

CRC Handbook of Basic Tables for Chemical Analysis


Author: Thomas J. Bruno,Paris D.N. Svoronos
Publisher: CRC Press
ISBN: 1420039911
Category: Science
Page: 688
View: 5359

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If you are a researcher in organic chemistry, chemical engineering, pharmaceutical science, forensics, or environmental science, you make routine use of chemical analysis. And like its best-selling predecessor was, the Handbook of Basic Tables for Chemical Analysis, Second Edition is your one-stop source for the information needed to design chemical analyses. Here's what is new in the Second Edition: New chapters on solutions, electroanalytical methods, electrophoresis, and laboratory safety An expanded section on gas chromatography that includes data on compounds that attack common detectors New information on detector optimization An updated section on high performance liquid chromatography that provides the most recent chiral stationary phases, detector information, and revised solvent tables Updated information on the most useful "wet" chemistry methods Enlarged section of Miscellaneous Tables Going far beyond the landmark first edition in terms of scope and applications, the second edition provides current and updated data culled from a wide range of resources and consolidated into a concise yet easy-to-use format. The book's laser-like focus on core information gives you the knowledge you need when you need it - at the decision point.